Microstructure and Phase Composition of Cold Isostatically Pressed and Pressureless Sintered Silicon Nitride.

نویسندگان

  • O A Lukianova
  • V V Krasilnikov
  • A A Parkhomenko
  • V V Sirota
چکیده

The microstructure and physical properties of new Y2O3 and Al2O3 oxide-doped silicon nitride ceramics fabricated by cold isostatic pressing and free sintering were investigated. The phase composition of produced material was also studied by X-ray diffraction at room and elevated temperature. The fabricated ceramics featured a microstructure of Si5AlON7 grains with a fine-grained α-Si3N4 with a small amount of Y2SiAlON5. Described ceramics is attractive for many high-temperature structural applications due to beneficial combination of fine-grained structure with improved mechanical properties and small weight loss.

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

منابع مشابه

Effect of Silicon Carbide and graphite additives on the pressureless Sintering mechanism and microstructural characteristics of Ultra-High Temperature ZrB2 Ceramics Composites

The effect of SiC content, additives, and process parameters on densification and microstructural properties of pressureless sintered ZrB2– (1–10 wt %) SiC particulate composites have been studied. The ZrB2–SiC composite powders mixed by Spex mixer with 1-2wt% C (added as graphite powder) and CMC have been cold-compacted and sintered in argon environment in the temperature range of 1800–2100ºC ...

متن کامل

Microstructure of Spark Plasma-Sintered Silicon Nitride Ceramics

The microstructure and phase composition of the high-content Al2O3-Y2O3-doped spark plasma-sintered silicon nitride were investigated. Fully dense silicon nitride ceramics with a typical α-Si3N4 equiaxed structure with average grain size from 200 to 530 nm, high elastic modulus of 288 GPa, and high hardness of 2038 HV were spark plasma sintered (SPSed) at 1550 °C. Silicon nitride with elongated...

متن کامل

Structural and Electrical Characterization of Sintered Silicon Nitride Ceramic

The electrical conduction phenomena, dielectric response and microstructure have been discussed in sintered silicon nitride ceramics at different temperature and frequencies. Microstructure and phase of the sintered samples was investigated by Scanning Electron Microscope (SEM) and X-ray diffractometer (XRD). The electrical conductivity, dielectric constant and dielectric loss increases exponen...

متن کامل

Low Temperature Sintering Additives for Silicon Nitride

This work deals with sintering additives for the low temperature pressureless sintering of Si3N4, via a transient liquid technique. Much attention has been given to the development of a sintering process using low-cost Si3N4 powder (Silzot HQ, Germany) as the starting material and employing sintering additives which are also both economically attractive and enable sintering at low temperatures....

متن کامل

The microstructure and boundary phases of in-situ reinforced silicon nitride

The microstructure of an in-situ reinforced silicon nitride, gas pressure sintered with La2O3, Y2O3, and SrO additives and then heat treated, is examined with X-ray diffraction, SEM, and high-resolution TEM. Two crystalline rare-earth apatite phases, La5Si3O12N and Y5Si3O12N, are identified at the grain pockets and at the two-grain boundaries. The thickness of the crystalline phases at the two-...

متن کامل

ذخیره در منابع من


  با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید

برای دانلود متن کامل این مقاله و بیش از 32 میلیون مقاله دیگر ابتدا ثبت نام کنید

ثبت نام

اگر عضو سایت هستید لطفا وارد حساب کاربری خود شوید

عنوان ژورنال:
  • Nanoscale research letters

دوره 11 1  شماره 

صفحات  -

تاریخ انتشار 2016